什么是
原位
显微术？
原位
透射电子显微术将透射电子显微镜 (TEM) 的成像能力与某些外部激源的加载相结合以观察样品的实时动态过程。 目前，有许多种系统和样品杆可以用来对样品施加不同的外场刺激来研究在偏压、机械应变/变形、加热、冷却、气体或液体环境的引入或仅仅是强电子束辐照状况下的动态过程。
过去，各种反应和系统动力学信息可记录在录像带上。在此基础上，截屏程序的出现，能够记录低分辨率的定性视频，使您能够以视频帧率，例如以30帧/秒（fps）的速度，来可视化反应情况。
现在，随着数据传输速度和数据处理能力的提升，配备了Gatan的原位相机，您可以直接对传感器输出来进行大规模数据集的记录和管理。在一次原位实验中，利用原位相机捕获的每一帧原始、定量的数据，都能被直接存储到磁盘，并以单帧图像或可回放视频的形式进行处理。此外，各种算法或脚本（例如求和、漂移校正、像素合并等）能够对采集数据进行后处理，以提取数据中的有用部分，例如下面视频所示。Gatan原位相机附带的内建管理工具使您能够轻松的对数据进行分离和提取，从而对处理后的数据进行分析，来对加载于系统的刺激导致的效应进行定量化。这一数据采集和后处理的工作流程大大提高了一次电镜机时中能够进行的实验数量。同时这一提升也使得以前无法达到的时间与空间分辨率成为可能，亚毫秒的时间分辨率，使得对于以前来说发生太快的反应能够被采集，也使得以前不为人知的动态过程得以解析。
该数据显示了Gatan OneView
®
IS相机与DENSsolutions Wildfire加热杆在1300
°C下互相配合的稳定性。以优异空间与时间分辨率捕获到紧随温度变化发生的颗粒形貌变化过程。我们无法先验的知道到底哪个（或哪些）颗粒将发生变化，但由于OneView IS相机的大视场，这些颗粒都能够被以同样的空间分辨率同时记录下来。
主视频以10倍速率进行回放，而颗粒形状变化的回放速度为2倍。内插视频进行了放大，以显示晶格条纹的解析。
该视频未进行过漂移校正或剪裁。视频进行了帧叠加平均以提高信噪比。样品：SiO
2
上的Ru
SiNx上蒸镀的Au薄膜的烧结过程由Gatan Rio™ 16 IS（原位）相机拍摄。样品通过DENSsolutions Wildfire加热杆加热到650 °C。该视频通过Gatan Microscopy Suite
®
软件的IS player进行了漂移校正与裁剪。
该数据显示了在CeO
2
纳米颗粒表面单独原子柱的运动状况，以400 fps记录。这一运动是由室温下电子束的辐照所引起的。K2
®
IS相机的时间分辨率使得这一运动过程能够得到观察。
该视频以两个不同的速度进行回放（真实速度的1/2和1/10），使得该视频中显著发生原子柱运动的部分以更慢的速度进行回放以体现细节。即便在慢速的部分，也进行了跳帧处理，因为该视频的帧率为30 fps，而原始数据的1/10速度为40 fps。
该视频进行了漂移校正、背底扣除、图像过滤与裁剪。
The team at the
Nanomaterials, Mechanics, and MEMS Laboratory
is focused on the synthesis and characterization of...
Department of Materials Science and Engineering.
School for the Engineering of Matter, Transport, and Energy. Arizona State University (ASU)
Intermetallic nanocrystal discovery through modulation of atom stacking hierarchy
Du, J. S.; Dravid, V. P.; Mirkin, C. A.
How to get something out of nothing (almost!): Extracting information from noisy data
Microscopy and Microanalysis
Time-resolved imaging of stochastic cascade reactions over a submillisecond to second time range at the angstrom level
Journal of American Chemical Society
Shimizu, T.; Lungerich, D.; Harano, K.; Nakamura, E.
Polymer-stabilized Au38 cluster: Atomically precise synthesis by digestive ripening and characterization of atomic structure and oxidation catalysis
Hasegawa, S.; Masuda, S.; Takano, S.; Harano, K.; Tsukuda, T.
Metastable hexagonal close-packed palladium hydride in liquid cell TEM
Hong, J.; Bae, J. -H.; Jo, H.; Park, H. -Y.; Lee, S.; Hong, S. J.; Chun, H.; Cho, M. K.; Kim, J.; Kim, J.; Son, Y.; Jin, H.; Suh, J. -Y.; Kim, S. -C.; Roh, H. -K.; Lee, K. H.; Kim, H. -S.; Chung, K. Y.; Yoon, C. W.; Lee, K.; Kim, S. H.; Ahn, J. -P.; Baik, H.; Kim, G. H.; Han, B.; Jin, S.; Hyeon, T.; Park, J.; Son, C. Y.; Yang, Y.; Lee, Y. -S.; Yoo, S. J.; Chun, D. W.
Electron microscopy for polymer structures
Ionization and electron excitation of C60 in a carbon nanotube: A variable temperature/voltage transmission electron microscopic study
Liu, D.; Kowashi, S.; Nakamuro, T.; Lungerich, D.; Yamanouchi, K.; Harano, K.; Nakamura, E.
Graphene coating on silicon anodes enabled by thermal surface modification for high-energy lithium-ion batteries
Kim, S. C.; Huang, W.; Zhang, Z.; Wang, J.; Kim, Y.; Jeong, Y. K.; Oyakhire, S. T.; Yang, Y.; Cui, Y.
Lattice-resolution, dynamic imaging of hydrogen absorption into bimetallic AgPd nanoparticles
Angell, D. K.; Bourgeois, B.; Vadai, M.; Dionne, J. A.
Suspension electrolyte with modified Li+ solvation environment for lithium metal batteries
Kim, M. S.; Zhang, Z.; Rudnicki, P. E.; Yu, Z.; Wang, J.; Wang, H.; Oyakhire, S. T.; Chen, Y.; Kim, S. C.; Zhang, W.; Boyle, D. T.; Kong, X.; Xu, R.; Huang, Z.; Huang, W.; Bent, S. F.; Wang, L. -W.; Qin, J.; Bao, Z.; Cui , Y.
Rational solvent molecule tuning for high-performance lithium metal battery electrolytes
Yu, Z.; Rudnicki, P. E.; Zhang, Z.; Huang, Z.; Celik, H.; Oyakhire, S. T.; Chen, Y.; Kong, X.; Kim, S. C.; Xiao, X.; Wang, H.; Zheng, Y.; Kamat, G. A.; Kim, M. S.; Bent, S. F.; Qin, J.; Cui, Y.; Bao, Z.
Capturing the swelling of solid-electrolyte interphase in lithium metal batteries
Zhang, Z.; Li, Y.; Xu, R.; Zhou, W.; Li, Y.; Oyakhire, S. T.; Wu, Y.; Xu, J.; Wang, H.; Yu, Z.; Boyle, D. T.; Huang, W.; Ye, Y.; Chen, H.; Wan, J.; Bao, Z.; Chiu, W.; Cui, Y.
Capturing the swelling of solid-electrolyte interphase in lithium metal batteries
Zhang, Z.; Li, Y.; Xu, R.; Zhou, W.; Li, Y.; Oyakhire, S. T.; Wu, Y.; Xu, J.; Wang, H.; Yu, Z.; Boyle, D. T.; Huang, W.; Ye, Y.; Chen, H.; Wan, J.; Bao, Z.; Chiu, W.; Cui, Y.
Electric field control of chirality
Behera, P.; May, M. A.; Gomez-Ortiz, F.; Susarla, S.; Das, S.; Nelson, C. T.; Caretta, L.; Hsu, S. -L.; McCarter, M. R.; Savitzky, B. H.; Barnard, E. S.; Raja, A.; Hong, Z.; Garcia-Fernandez, P.; Lovesey, S. W.; Van der Laan, G.; Ercius, P.; Ophus, C.; Martin, L. W.; Junquera, J.; Raschke, M. B.; Ramesh, R.
De novo synthesis of free-standing flexible 2-D intercalated nanofilm uniform over tens of cm2
Ravat, P.; Uchida, H.; Sekine, R.; Kamei, K.; Yamamoto, A.; Konovalov, O.; Tanaka, M.; Yamada, T.; Harano, K.; Nakamura, E.
Spatial mapping of electrostatic fields in 2D heterostructures
Murthy, A. A.; Ribet, S. M.; Stanev, T. K.; Liu, P.; Watanabe, K.; Taniguchi, T.; Stern, N. P.; dos Reis, R.; Dravid, V. P.
Electron crystallographic investigation of crystals on the mesostructural scale
Microscopy and Microanalysis
Mao, W.; Bao, C.; Han, L.
Atomic-number (Z)-correlated atomic sizes for deciphering electron microscopic molecular images
Xing, J.; Takeuchi, K.; Kamei, K.; Nakamuro, T.; Harano, K.; Nakamura, E.
Nanodiffraction imaging of polymer crystals
Kanomi, S.; Marubayashi, H.; Miyata, T.; Tsuda, K.; Jinnai, H.
In-situ transmission electron microscopy observation of the helium bubble evolution in pre-irradiated fluorapatite during annealing
Lin, Z.; Wu, C.; He, H.; Jiang, S.; Ren, F.; Cao, L.; Huang, Z.; Zhang, J.
Local chemical fluctuation mediated ductility in body-centered-cubic high-entropy alloys
Bu, Y.; Wu, Y.; Lei, Z.; Yuan, X.; Wu, H.; Feng, X.; Liu, J.; Ding, J.; Lu, Y.; Wang, H.; Lu, Z.; Yang, W.
A singular molecule-to-molecule transformation on video: The bottom-up synthesis of fullerene C60 from truxene derivative C60H30
Lungerich, D.; Hoelzel, H.; Harano, K.; Jux, N.; Amsharov, K. Y.; Nakamura, E.
Intrinsic helical twist and chirality in ultrathin tellurium nanowires
Londoño-Calderon, A.; Williams, D. J.; Schneider, M. M.; Savitzky, B. H.; Ophus, C.; Ma, S.; Zhud, H.; Pettes, M. T.
Direct visualization of the earliest stages of crystallization
Microscopy and Microanalysis
Singh, M. K.; Ghosh, C.; Miller, B.; Carter, C. B.
Dual-solvent Li-ion solvation enables high-performance Li-metal batteries
Wang, H.; Yu, Z.; Kong, X.; Huang, W.; Zhang, Z.; Mackanic, D. G.; Huang, X.; Qin, J.; Bao, Z.; Cui. Y.
An in-situ TEM study into the role of disorder, temperature and ballistic collisions on the accumulation of helium bubbles and voids in glass-ceramic composites
Journal of Nuclear Materials
Mir, A. H.; Hyatt, N. C.; Donnelly, S. E.
New magic Au24 cluster stabilized by PVP: Selective formation, atomic structure, and oxidation catalysis
Hasegawa, S.; Takano, S.; Harano, K.; Tsukuda, T.
New magic Au24 cluster stabilized by PVP: Selective formation, atomic structure and oxidation catalysis
Hasegawa, S.; Takano, S.; Harano, K.; Tsukuda, T.
Rim binding of cyclodextrins in size-sensitive guest recognition
Journal of American Chemical Society
Hanayama, H.; Yamada, J.; Tomotsuka, I.; Harano, K.; Nakamura, E.
Corrosion of lithium metal anodes during calendar ageing and its microscopic origins
Boyle, D. T.; Huang, W.; Wang, H.; Li, Y.; Chen, H.; Yu, Z.; Zhang, W.; Bao, Z.; Cui, Y.
Few-nm-sized, phase-pure Au5Sn intermetallic nanoparticles: synthesis and characterization
Osugi, S.; Takano, S.; Masuda, S.; Harano, K.; Tsukuda, T.
Mapping grains, boundaries, and defects in 2D covalent organic framework thin films
Castano, I.; Evans, A. M.; dos Reis, R,; Dravid, V. P.; Gianneschi, N. C.; Dichtel, W. R.
Nano- and microspheres containing inorganic and biological nanoparticles: Self-assembly and electron tomographic analysis
Journal of American Chemical Society
Sekine, R.; Ravat, P.; Yanagisawa, H.; Liu, C.; Kikkawa, M.; Harano, K.; Nakamura, E.
SINGLE: Atomic-resolution structure identification of nanocrystals by graphene liquid cell EM
Reboul, C. F.; Heo, J.; Machello, C.; Kiesewetter, S.; Kim, B. H.; Kim, S.; Elmlund, D.; Ercius, P.; Park, J.; Elmlund, H.
Capturing the moment of emergence of crystal nucleus from disorder
Journal of American Chemical Society
Nakamuro, T.; Sakakibara, M.; Nada, H.; Harano, K.;Nakamura, E.
4D imaging of soft matter in liquid water
Marchello, G.; De Pace, C.; Acosta-Gutierrez, S.; Lopez-Vazquez, C.; Wilkinson, N.; Gervasio, F. L.; Ruiz-Perez, L.; Giuseppe Battaglia, G.
Spatial mapping of electrostatics and dynamics across 2D heterostructures
Murthy, A. A.; Stanev, T. K.; Ribet, S. M.; Liu, P.; Watanabe, K.; Taniguchi, T.; Stern, N. P.; dos Reis, R.; Dravid, V. P.
Electronically coupled 2D polymer/MoS2 heterostructures
Journal of American Chemical Society
Balch, H. B., Evans, A. M., Dasari, R. R., Li, H., Li, R., Thomas, S., Wang, Q., Bisbey, R. P., Slicker, K., Castano, I., Xun, S., Jiang, L., Zhu, C., Gianneschi, N., Ralph, D. C., Brédas, J-L., Marder, S. R., Dichtel, W. R., Wang, F.
Cathode-electrolyte interphase in lithium batteries revealed by cryogenic electron microscopy
Zhang, Z.; Yang, J.; Huang, W.; Wang, H.; Zhou, W.; Li, Y.; Li, Y.; Xu, J.; Huang, W.; Chiu, W.
Synthesis and characterization of a well-defined carbon nanohorn-supported molybdenum dioxo catalyst by SMART-EM imaging. Surface structure at the atomic level
Bulletin of the Chemical Society of Japan
Kratish, Y.; Nakamuro, T.; Liu, Y.; Li, J.; Tomotsuka, I.; Harano, K.; Nakamura, E.; Marks, T. J.
Imaging arrangements of discrete ions at liquid−solid interfaces
Li, H. -K.; de Souza, J. P.; Zhang, Z.; Martis, J.; Sendgikoski, K.; Cumings, J.; Bazant, M. Z.; Majumdar, A.
In situ TEM study of crystallization and chemical changes in an oxidized uncapped Ge2Sb2Te5 film
Journal of Applied Physics
Singh, M. K.; Ghosh, C.; Miller, B.; Kotula, P. G.; Tripathi, S.; Watt, J.; Bakan, G.; Silva, H.; Carter, C. B.
Inside polyMOFs: Layered structures in polymer-based metal–organic frameworks
Bentz, K. C., Gnanasekaran, K., Bailey, J. B. Ayala, S., Tezcan, F. A., Gianneschi, N. C., Cohen, S. M.
Aryl radical addition to curvatures of carbon nanohorns for single-molecule level molecular imaging
Bulletin of the Chemical Society of Japan
Kamei, K.; Shimizu, T.; Harano, K.; Nakamura, E.
Light-induced anisotropic morphological dynamics of black phosphorus membranes visualized by dark-field ultrafast electron microscopy
Kim, Y. -J.; Lee, Y.; Kim, K.; Kwon, O. -H.
Effect of adventitious carbon on pit formation of monolayer MoS2
Park, S.; Siahrostami, S.; Park, J.; Mostaghimi, A. H. B.; Kim, T. R.; Vallez, L.; Gill, T. M.; Park, W.; Goodson, K. E.; Sinclair, R.; Zheng, X.
Ultra-fast electron microscopic imaging of single molecules with direct electron detection camera and noise reduction
Microscopy and Microanalysis
Stuckner, J.; Shimizu, T.; Harano, K.; Nakamura, E.; Murayama, M.
In situ monitoring of the seeding and growth of silver metal–organic nanotubes by liquid-cell transmission electron microscopy
Gnanasekaran, K., Vailonis, K. M., Jenkins, D. M., Gianneschi, N. C.
Real-time video imaging of mechanical motions of a single molecular shuttle with sub-millisecond sub-angstrom precision
Bulletin of the Chemical Society of Japan
Shimizu, T.; Lungerich, D.; Stuckner, J.; Murayama, M.; Harano, K.; Nakamura, E.
Cyclodextrins as surfactants for solubilization and purification of carbon nanohorn aggregates
Chemistry, an Asian Journal
Hanayama, H.; Yamada, J.; Harano, K.; Nakamura, E.
Decoding the stoichiometric composition and organisation of bacterial metabolosomes
Yang, M.; Simpson, D. M.; Wenner, N.; Brownridge, P.; Harman, V. M.; Hinton, J. C. D.; Beynon, R. J.; Liu , L. -N.
1D to 2D transition in tellurium observed by 4D electron microscopy
Londoño-Calderon, A.; Williams, D. J.; Ophus, C.; Pettes, M. T.
Direct visualization of electric-field-induced structural dynamics in monolayer transition metal dichalcogenides
Murthy, A. A.; Stanev, T. K.; dos Reis, R.; Hao, S.; Wolverton, C.; Stern, N. P.; Dravid, V. P.
Unveiling the microscopic origins of phase transformations: An in situ TEM perspective
Yu, L.; Hudak, B. M.; Ullah, A.; Thomas, M. P.; Porter, C. C.; Thisera, A.; Pham, R. H.; Goonatilleke, M. D. A.; Guiton, B. S.
Direct observation of amorphous precursor phases in the nucleation of protein–metal–organic frameworks
Journal of American Chemical Society
Ogata, A. F.; Rakowski, A. M.; Carpenter, B. P.; Fishman, D. A.; Merham, J. G.; Hurst, P. J.; Patterson, J. P.
Hybrid nanocellulose decorated with silver nanoparticles as reinforcing filler with antibacterial properties
Materials Science and Engineering: C
Errokh, A.; Magnin, A.; Putaux, J. -L.; Boufi, S.
Conductive 2D metal-organic framework for high-performance cathodes in aqueous rechargeable zinc batteries
Nam, K. W.; Park, S. S.; dos Reis, R.; Dravid, V. P. Kim, H.; Mirkin, C. A.; Stoddart, J. F.
Real-space charge-density imaging with sub-ångstrom resolution by four-dimensional electron microscopy
Gao, W.; Addiego, C.; Wang, H,; Yan, X.; Hou, Y.; Ji, D.; Heikes, C.; Zhang, Y.; Li, L.; Huyan, H.; Blum, T.; Aoki, T.; Nie, Y.; Schlom, D.; Wu, R.; Pan, X.
Large piezoelectric coefficient with enhanced thermal stability in Nb5+-doped Ba0.85Ca0.15Zr0.1Ti0.9O3 ceramics
He, L.; Ji, Y.; Ren, S.; Zhao, L.; Luo, H.; Liu, C.; Hao, Y.; Zhang, L.; Zhang, L.; Ren, X.
Recent progress of in situ transmission electron microscopy for energy materials
Atomistic structures and dynamics of prenucleation clusters in MOF-2 and MOF-5 syntheses
Xing, J.; Schweighauser, L.; Okada, S.; Harano, K.; Nakamura, E.
Quantifying inactive lithium in lithium metal batteries
Fang, C.; Li, J.; Zhang, M.; Zhang, Y.; Yang, F.; Lee, J. Z.; Lee, L. M. -H.; Alvarado, J.; Schroeder, M. A.; Yang, Y.; Lu, B.; Williams, N.; Ceja, M.; Yang, L.; Cai, M.; Gu, J.; Xu, K.; Wang, X.; Meng, Y. S.
Formation of two-dimensional transition metal oxide nanosheets with nanoparticles as intermediates
Yang, J.; Zeng, Z.; Kang, J.; Betzler, S.; Czarnik, C.; Zhang, X.; Ophus, C.; Yu, C.; Bustillo, K.; Pan, M.; Qiu, J.; Wang, L. -W.; Zheng, H.
Probing the degradation of carbon nanotubes in aqueous solution by liquid cell transmission electron microscopy
Wang, H.; Liu, Z.; Liu, H.; Guan, L.; Cao, X.; Zhang, Z.; Huang, Y.; Jin, C.
Monolayer Ti3C2Tx as an effective co-catalyst for enhanced photocatalytic hydrogen production over TiO2
ACS Applied Energy Material
Su, T.; Hood, Z. D.; Naguib, M.; Bai, L.; Luo, S.; Rouleau, C. M.; Ivanov, I. N.; Ji, H.; Qin, Z.; Wu, Z.
Thermal stability and irradiation response of nanocrystalline CoCrCuFeNi high-entropy alloy
Zhang, Y.; Tunes, M. A.; Crespillo, M. L.; Zhang, F.; Boldman, W. L.; Rack, P. D.; Jiang, L.; Xu, C.; Greaves, G.; Donnelly, S. E.; Wang, L.; Weber, W. J.
Site-selective CO disproportionation mediated by localized surface plasmon resonance excited by electron beam
Yang, W. -C. D.; Wang, C.; Fredin, L. A.; Lin, P. A.; Shimomoto, L.; Lezec, H. J.; Sharma, R.
Off-axis electron holography for imaging the magnetic behavior of vortex-state minerals
Almeida, T. P.; Muxworthy, A. R.; Williams, W.; Kasama, T.; Kovács, A.; Dunin-Borkowski, R. E.
Mechanical response of gasoline soot nanoparticles under compression: An in situ TEM study
Jenei, I. Z.; Dassenoy, F.; Epicier, T.; Khajeh, A.; Martinic, A.; Uy, D.; Ghaednia, H.; Gangopadhyay, A.
Attapulgite-CeO2/MoS2 ternary nanocomposite for photocatalytic oxidative desulfurization
Li, X.; Zhang, Z.; Yao, C.; Lu, X.; Zhao, X.; Ni, C.
Nanoscale mosaicity revealed in peptide microcrystals by scanning electron nanodiffraction
Gallagher-Jones, M.; Ophus, C.; Bustillo, K. C.; Boyer, D. R.; Panova, O.; Glynn, C.; Zee, C., -T.; Ciston, J.; Mancia, K. C.; Minor, A. M.; Rodriguez, J. A.
Surface crystallization of liquid Au–Si and its impact on catalysis
Panciera, F.; Tersoff, J.; Gamalski, A. D.; Reuter, M. C.; Zakharov, D.; Stach, E. A.; Hofmann, S.; Ross, F. M
Layered-structure SbPO4/reduced graphene oxide: An advanced anode material for sodium ion batteries
Pan, J.; Chen, S.; Fu, Q.; Sun, Y.; Zhang, Y.; Lin, N.; Gao, P.; Yang, J.; Qian, Y.
In situ protein micro-crystal fabrication by cryo-FIB for electron diffraction
Li, X.; Zhang, S.; Zhang, J.; Sun, F.
Dynamics of transformation from platinum icosahedral nanoparticles to larger FCC crystal at millisecond time resolution
Gao, W.; Wu, J.; Yoon, A.; Lu, P.; Qi, L.; Wen, J.; Miller, D. J.; Mabon, J. C.; Wilson, W. L.; Yang, H.; Zuo, J. -M.
Atomic step flow on a nanofacet
Harmand, J. -C.; Patriarche, G.; Glas, F.; Panciera, F.; Florea, I.; Maurice, J. -L.; Travers, L.; Ollivier, Y.
A high-entropy alloy with hierarchical nanoprecipitates and ultrahigh strength
Fu, Z.; Jiang, L.; Wardini, J. L.; MacDonald, B. E.; Wen, H.; Xiong, W.; Zhang, D.; Zhou, Y.; Rupert, T. J.; Chen, W.; Lavernia, E. J.
SnP2O7 covered carbon nanosheets as a long‐life and high‐rate anode material for sodium‐ion batteries
Advanced Functional Materials
Pan, J.; Chen, S.; Zhang, D.; Xu, X.; Sun, Y.; Tian, F.; Gao, P.; Yang, J.
Stability of halide perovskite solar cell devices: In situ observation of oxygen diffusion under biasing
Jung, H. J.; Kim, D.; Kim, S.; Park, J.; Dravid, V. P.; Shin, B.
In situ kinetic and thermodynamic growth control of Au–Pd core–shell nanoparticles
Journal of American Chemical Society
Tan, S. F.; Bisht, G.; Anand, U.; Bosman, M.; Yong, X. E.; Mirsaidov, U.
Probing light atoms at sub-nanometer resolution: Realization of scanning transmission electron microscope holography
Cornell University Library
Yasin, F. S.; Harvey, T. R.; Chess, J. J.; Pierce, J. S.; Ophus, C.; Ercius, P.; McMorran, B. J.
Correlation between electrical transport and nanoscale strain in InAs/In0.6Ga0.4As core–shell nanowires
Zeng, L.; Gammer, C.; Ozdol, B.; Nordqvist, T.; Nygård, J.; Krogstrup, P.; Minor, A. M.; Jäger, W.; Olsson, E.
In situ observation of resistive switching in an asymmetric graphene oxide bilayer structure
Kim, S.; Jung, H. J.; Kim, J. C.; Lee, K. -S.; Park, S. S.; Dravid, V. P.; He, K.; Jeong, H. Y.
Fast gas–solid reaction kinetics of nanoparticles unveiled by millisecond in situ electron diffraction at ambient pressure
Yu, J.; Yuan, W.; Yang, H.; Xu, Q.; Wang, Y.; Zhang, Z.
Local nanoscale strain mapping of a metallic glass during in situ testing
Gammer, C.; Ophus, C.; Pekin, T. C.; Eckert, J.; Minor, A. M.
Highly reversible oxygen-redox chemistry at 4.1 V in Na4/7-x[square Mn-1/7(6/7)]O-2 (square: Mn vacancy)
Advanced Energy Materials
de Boisse, B. M.; Nishimura, S.; Watanabe, E.; Lander, L.; Tsuchimoto, A.; Kikkawa, J.; Kobayashi, E.; Asakura, D.; Okubo, M.; Yamada, A.
Crystallization behavior of the Li2S–P2S5 glass electrolyte in the LiNi1/3Mn1/3Co1/3O2 positive electrode layer
Tsukasaki, H.; Mori, Y.; Otoyama, M.; Yubuchi, S.; Asano, T.; Tanaka, Y.; Ohno, T.; Mori, S.; Hayashi, A.; Tatsumisago, M.
Facile synthesis and superior catalytic activity of nano-TiN@N–C for hydrogen storage in NaAlH4
ACS Applied Materials and Interfaces
Zhang, X.; Ren, Z.; Lu, Y.; Yao, J.; Gao, M.; Liu, Y.; Pan, H.
Ionic conductivity and crystallization process in the Li2S–P2S5 glass electrolyte
Tsukasaki, H.; Mori, S.;Shiotani, S.; Yamamura, H.
Nanoparticle interactions guided by shape‐dependent hydrophobic forces
Tan, S. F.; Raj, S.; Bisht, G.; Annadata, H. V.; Nijhuis, C. A.; Král, P.; Mirsaidov, U.
Mapping thermal expansion coefficients in freestanding 2D materials at the nanometer scale
Hu, X.; Yasaei, P.; Jokisaari, J.; Öğüt, S.; Salehi-Khojin, A.; Klie, R. F.
Evolving affinity between Coulombic reversibility and hysteretic phase transformations in nano-structured silicon-based lithium-ion batteries
Ogata, K.; Jeon, S.; Ko, D.-S.; Jung, I. S.; Kim, J. H.; Ito, K.; Kubo, Y.; Takei, K.; Saito, S.; Cho, Y.-H.; Park, H.; Jang, J.; Kim, H.-G.; Kim, J. -H.; Kim, Y. S.; Choi, W.; Koh, M.; Uosaki, K.; Doo, S. G.; Hwang, Y.; Han, S.
Solvent-free and biocompatible multiphased organic–inorganic hybrid nanocomposites
da Silva, L. C. E.; Germiniani, L. G. L.; Plivelic, T. S.; Gonçalves, M. C.
Creation of single chain of nanoscale skyrmion bubbles with record-high temperature stability in a geometrically confined nanostripe
Hou, Z.; Zhang, Q.; Xu, G.; Gong, C.; Ding, B.; Wang, Y.; Li, H.; Liu, E.; Xu, F.; Zhang, H.; Yao, Y.; Wu, G.; Zhang, X. - X.; Wang, W.
First transparent oxide ion conducting ceramics synthesized by full crystallization from glass
Journal of Materials Chemistry A
Boyer, M.; Yang, X.; Carrión, A. J. F.; Wang, Q.; Véron, E.; Genevois, C.; Hennet, L.; Matzen, G.; Suard, E.; Thiaudière, D.; Castro, C.; Pelloquin, D.; Kong, L. B.; Kuang, X.; Allix, M.
Direct microscopic analysis of individual C60 dimerization events: Kinetics and mechanisms
Journal of American Chemical Society
Okada, S.; Kowashi, S.; Schweighauser, L.; Yamanouchi, K.; Harano, K.; Nakamura, E.
Analysis of structural and thermal stability in the positive electrode for sulfide-based all-solid-state lithium batteries
Tsukasaki, H.; Otoyama, M.; Mori, Y.; Mori, S.; Morimoto, H.; Hayashi, A.; Tatsumisago, M.
Atomic structure of sensitive battery materials and interfaces revealed by cryo–electron microscopy
Li, Y.; Li.; Y.; Pei, A.; Yan, K.; Sun, Y.; Wu, C. -L; Joubert, L. -M.; Chin, R.; Koh, A. L.; Yu, Y.; Perrino, J.; Butz, B.; Chu, S.; Cui, Y.
Magnetic antiskyrmions above room temperature in tetragonal Heusler materials
Nayak, A. K.; Kumar, V.; Ma, T.; Werner, P.; Pippel, E.; Sahoo, R.; Damay, F.; Rößler, U. K.; Felser, C.; Parkin, S. S. P.
High temperature-stability of (Pb 0.9 La 0.1 )(Zr 0.65 Ti 0.35 )O 3 ceramic for energy-storage applications at finite electric field strength
Gao, J.; Liu, Y.; Wang, Y.; Wang, D.
A discovery of strong metal–support bonding in nanoengineered Au–Fe3O4 dumbbell-like nanoparticles by in situ transmission electron microscopy
Han, C. W.; Choksi, T.; Milligan, C.; Majumdar, P.; Manto, M.; Cui, Y.; Sang, X.; Unocic, R. R.; Zemlyanov, D.; Wang, C.; Ribeiro, F. H.; Greeley, J.; Ortalan, V.
Direct observation of a non-crystalline state of Li2S–P2S5 solid electrolytes
Tsukasaki, H.; Mori, S.; Morimoto, H.; Hayashi, A.; Tatsumisago , M.
In situ observation of twin boundary sliding in single crystalline Cu nanowires
Yue, Y.; Zhang, Q.; Zhang, X.; Yang, Z.; Yin, P.; Guo, L.
Investigation of thermal stability of P2–NaxCoO2 cathode materials for sodium ion batteries using real-time electron microscopy
ACS Applied Materials and Interfaces
Hwang, S.; Lee, Y.; Jo, E.; Chung, K. Y.; Choi, W.; Kim, S. M.; Chang, W.
Vertical graphene growth on SiO microparticles for stable lithium ion battery anodes
Shi, L.; Pang, C.; Chen, S.; Wang, M.; Wang, K.; Tan, Z.; Gao, P.; Ren, J.; Huang. Y.; Peng, H.; Liu, Z.
Shape-controlled metal-free catalysts: Facet-sensitive catalytic activity induced by the arrangement pattern of noncovalent supramolecular chains
Geng, G.; Chen, P.; Guan, B.; Jiang, L.; Xu, Z.; Di, D.; Tu, Z.; Hao, W.; Yi, Y.; Chen, C.; Liu, M.; Hu, W.
Secondary phases in AlxCoCrFeNi high-entropy alloys: An in-situ TEM heating study and thermodynamic appraisal
Rao, J. C.; Diao, H. Y.; Ocelík, V.; Vainchtein, D.; Zhang, C.; Kuo, C.; Tang, Z.; Guo, W.; Poplawsky, J. D.; Zhou, Y.; Liaw, P. K.; De Hosson, J. Th. M.
Origin of zero and negative thermal expansion in severely-deformed superelastic NiTi alloy
Ahadi, A.; Matsushita, Y.; Sawaguchi, T.; Sun, Q. P.; Tsuchiya, K.
Non-spectroscopic composition measurements of SrTiO3-La0.7Sr0.3MnO3 multilayers using scanning convergent beam electron diffraction
Ophus, C.; Ercius, P.; Huijben, M.; Ciston, J.
Interlayer‐expanded vanadium oxychloride as an electrode material for magnesium‐based batteries
Minella, C. B.; Gao, P.; Zhao‐Karger, Z.; Mu, X.; Diemant, T.; Pfeifer, M.; Chakravadhanula, V. S. K.; Behm, R. J.; Fichtner, M.
Nanoscale engineering in VO2 nanowires via direct electron writing process
Zhang, Z.; Guo, H.; Ding, W.; Zhang, B.; Lu, Y.; Ke, X.; Liu, W.; Chen, F.; Sui, M.
Simple synthesis of highly uniform bilayer-carbon nanocages
Ziolkowska, D. A.; Jangam, J. S. Dilip; Rudakov, G.; Paronyan, T.; Akhtar, M.; Sumanasekera, G.; Jasinski, J. B.
Direct evidence of M2 phase during the monoclinic-tetragonal (rutile) phase transition of W-doped VO2 nanowires
Asayesh-Ardakani, H.; Yao, W.; Nie, A.; Marley, P. M.; Braham, E.; Klie, R. F.; Banerjee, S.; Shahbazian-Yassar, R.
Nanoscale iron nitride, ε-Fe3N: Preparation from liquid ammonia and magnetic properties
Zieschang, A. -M.; Bocarsly, J. D.; Dürrschnabel, M.; Molina-Luna, L.; Kleebe, H. -J.; Seshadri, R.; Albert, B.
Synthesis engineering of iron oxide raspberry-shaped nanostructures
Gerber, O.; Pichon, B. P.; Ihiawakrim, D.; Florea, I.; Moldovan, S.; Ersen, O.; Begin, D.; Grenèche, J. -M.; Lemonnier, S.; Barraud, E.; Begin-Colin, S.
The dissipation of field emitting carbon nanotubes in an oxygen environment as revealed by in situ transmission electron microscopy
Koh, A. L.; Gidcumb, E.; Zhou, O.; Sinclair, R.
Spatially resolved surface valence gradient and structural transformation of lithium transition metal oxides in lithium-ion batteries
Physical Chemistry Chemical Physics
Liu, H.; Bugnet, M.; Tessaro, M. Z.; Harris, K. J.; Dunham, M. J. R.; Jiang, M.; Goward, G. R.; Botton, G. A.
In situ XRD and TEM studies of sol-gel-based synthesis of LiFePO4
Crystal Growth and Design
Ziolkowska, D. A.; Jasinski, J. B.; Hamankiewicz, B.; Korona, K. P.; Wu, S. -H.; Czerwinsk, A.
Local and transient nanoscale strain mapping during in situ deformation
Gammer, C.; Kacher, J.; Czarnik, C.; Warren, O. L.; Ciston, J.; Minor, A. M.
The chemistry and structural thermal stability of hole-doped single crystalline SnSe
Journal of Alloys and Compounds
Zhang, B.; Peng, K.; Li, A.; Zhou, X.; Chen, Y.; Deng, Q.; Han, X.
Temperature and magnetic field dependence of the internal and lattice structures of skyrmions by off-axis electron holography
Shibata, K.; Kovács, A.; Kanazawa, N.; Dunin-Borkowski, R. E.; Tokura, Y.
Planar defect formation in the γ′ phase during high temperature creep in single crystal CoNi-base superalloys
Eggeler, Y. M.; Müller, J.; Titus, M. S.; Suzuki, A.; Pollock, T. M.; Spiecker, E.
Thermal stability comparison of nanocrystalline Fe-based binary alloy pairs
Journal of the Minerals, Metals & Materials Society
Clark, B. G.; Hattar, K. M.; Marshall, M. T.; Chookajorn, T.; Boyce, B. L.; Schuh, C. A.
Microstructure evolution and crystallography of the phase-change material TiSbTe films annealed in situ
Journal of Alloys and Compounds
Chen, Y. -J.; Zhang, B.; Ding, Q. -Q.; Deng, Q. -S.; Chen, Y.; Song, Z. -T.; Li, J. -X.; Zhang, Z.; Han, X. -D.
Revealing the formation of copper nanoparticles from a homogeneous solid precursor by electron microscopy
Journal of the American Chemical Society
van den Berg, R.; Elkjaer, C. F.; Gommes, C. J.; Chorkendorff, I.; Sehested, J.; de Jongh, P. E.; de Jong, K. P.; Helveg, S.
Highly mobile ferroelastic domain walls in compositionally graded ferroelectric thin films
Agar, J. C.; Damodaran, A. R.; Okatan, M. B.; Kacher, J.; Gammer, C.; Vasudevan, R. K.; Pandya, S.; Dedon, L. R.; Mangalam, R. V. K.; Velarde, G. A.; Jesse, S.; Balke, N.; Minor, A. M.; Kalinin, S. V.; Martin, L. W.
Direct observation of Σ7 domain boundary core structure in magnetic skyrmion lattice
Matsumoto, T.; So, Y. -G.; Kohno, Y.; Sawada, H.; Ikuhara, Y.; Shibata, N.
Strain mapping at nanometer resolution using advanced nano-beam electron diffraction
Ozdol, V. B.; Gammer,C.; Jin, X. G.; Ercius, P.; Ophus, C.; Ciston,J.; Minor, A. M.
In-situ study of the mechanisms of high temperature damage in elastic-plastic cyclic loading of nickel superalloy
Advanced Materials Research
Petrenec, M.; Polák, J.; Šamořil, T.; Dluhoš, J.; Obrtlík, K.
