Spectral data of tropical soils using dry-chemistry techniques (VNIR, XRF, and LIBS): a dataset for soil fertility prediction
Description
The dataset contains spectral data and characterizations of key soil fertility attributes of 102 soil samples. These samples are from two Brazilian agricultural areas, which have soils classified as Lixisol (Field 1) and Ferralsol (Field 2). Both type of soils are commonly found in Brazil’s tropical regions. The chosen fields have different soil matrices due to considerable textural and total elemental composition contrast. Regarding the fertility attributes, they present wide ranges of the variability of fertility attributes. After soil fertility tests, the samples were scanned with the following direct analysis techniques: (i) visible and near infrared diffuse reflectance spectroscopy (VNIR), (ii) X-ray fluorescence spectroscopy (XRF), and (iii) laser-induced breakdown spectroscopy (LIBS).
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Steps to reproduce
Soil samples were collected from 0 to 20 cm depth; oil fertility analyses for determining clay, organic matter (OM), cation exchange capacity (CEC), pH, base saturation (V), exchangeable (ex-) P, ex-K, ex-Ca, and ex-Mg were performed in a commercial laboratory. Loose soil samples (dry and grain size < 2mm) were scanned with the VNIR and XRF sensor. For LIBS data acquisition, the samples were pelletized after being comminuted (using a ball mill) with a binder material; Spectral data acquisition was performed under laboratory conditions after samples had been dried and sieved (≤ 2mm); The VNIR data was acquired after the spectrometer calibrates itself using reference materials with known spectral behaviour; For XRF data acquisition the X-ray tube was set for voltage and current of 35 kV and 7 μA, respectively. No vacuum condition or filters were used for the XRF spectra acquisition; For LIBS data acquisition, the following instrumental conditions were used: laser pulses with 65 mJ, 19.5 cm of lens-to-sample distance (given that 255 J cm−2 laser fluence), 15 accumulated laser pulses, 2 µs of delay time, and 7 µs of integration time gate.